1. please READ the question CAREFULY and answer EVERY PART. Tentatively identify the lower boiling solvent from the temperature of the first plateau and the ketone or alcohol from the temperature of the second plateau (the approximate boiling point of each component.) Examine the IR of the higher-boiling fraction and determine whether it is an alcohol or a ketone from the characteristic O-H, C=O, C-O stretch and C-Cl stretch. Identify which peak in the IR is from the âOH group of the alcohol or the C=O peak from the ketone. DRAW THE STRUCTURE OF THE COMPOUND.
2.Discuss qualitatively the effectiveness of the separation identifying peaks (if any) in the IR that appear to result from the lower boiling solvent
Analyst Date 3361 Thursday, October 12, 2017 3:28 PM 100 364899cm-1 95 2935.66cm-1 85 2886.39cm-1 1467.05 80- 1340 703.70cm-1 3337.04cm-1 28147c 1378.89cm-1 1275.9 110788ã_1 1 1604cm-1 816.64pm-1 65- 29 70.58cm-1 60- 1128.05cm-1 50 45- 950.46cm-1 38- 4000 2000 1500 1000 3500 3000 2500 650 cm-1 3361283 Sample 283 By 3361 Date Thursday, October 12 2017 ugher bonting purnt