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11 Nov 2019
Consider the chemical shifts, splitting patterns and relative numbers of each kind of hydrogen obtained from the proton NMR spectrum. Consider the chemical shifts and the number of peaks in the C-13 spectrum together with any other data supplied by the instructor (molecular formula, IR information, etc.) to determine the structure of each unknown. For each unknown, give a brief summary of your reasoning in the space provided below and draw a structure for the compound. If you are unable to determine the structure of the unknown, tell as much about the compound as possible. Draw the Lewis structure of each unknown on each of its spectra and clearly match each resonance with its respective hydrogen(s) and carbons. Label the NMR!
Fo0 .00 5.92 14 10 PPM FT-NMR red Fl:60.010 EX: acq.ppg IsWL: 1000 IPW: 168 usec OF1:378,3 INA: USER: Velin. Al -- DATE: 06/16/10 12:46) PTSid: 8192 Nuts - tcmp! IPD: 3.0 sec ILB: 0.0 Velin, Al, Valstie, :
Consider the chemical shifts, splitting patterns and relative numbers of each kind of hydrogen obtained from the proton NMR spectrum. Consider the chemical shifts and the number of peaks in the C-13 spectrum together with any other data supplied by the instructor (molecular formula, IR information, etc.) to determine the structure of each unknown. For each unknown, give a brief summary of your reasoning in the space provided below and draw a structure for the compound. If you are unable to determine the structure of the unknown, tell as much about the compound as possible. Draw the Lewis structure of each unknown on each of its spectra and clearly match each resonance with its respective hydrogen(s) and carbons. Label the NMR!
Fo0 .00 5.92 14 10 PPM FT-NMR red Fl:60.010 EX: acq.ppg IsWL: 1000 IPW: 168 usec OF1:378,3 INA: USER: Velin. Al -- DATE: 06/16/10 12:46) PTSid: 8192 Nuts - tcmp! IPD: 3.0 sec ILB: 0.0 Velin, Al, Valstie, :
Keith LeannonLv2
5 Mar 2019