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Please put the following steps in order for the general procedurefor testing anions. Be sure to clean and then rinse your teststubes with distilled water before starting, when you get a freshsample of anion solution or are done for the day. To determinewhich of the three possible cations (sodium, potassium, or lithium)are in the anion unknown you must do a flame test as was done inexperiment 2.

1 2 3 4 5 Finally dispose of all used chemicals in the waste bottlefor exp. 5 in the fume hood and wash glassware.

1 2 3 4 5 To anion solutions that form a precipitate with 0.1Msilver nitrate add 0.5 mL of 6M nitric acid, observe and mixwell.

1 2 3 4 5 Test the unknown for the anion analysis (5B-xxxx) usingthe same tests and logic used for the known anion solutions.

1 2 3 4 5 Test fresh samples of anion solutions that did not reactwith 6M HCl or 0.1M barium nitrate by adding 0.5 mL of 0.1M silvernitrate, observe and mix.

1 2 3 4 5 Observe while adding 0.5 mL of 6M HCl to 1 mL samples ofthe anion solutions and then add 5 drops of 0.1M barium nitrate andobserve again.

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Sixta Kovacek
Sixta KovacekLv2
28 Sep 2019
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