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18 Nov 2019
Solve the following holistic problem listing everything on the following checklist
General Checklist for Holistic Structure Problems (there are always exceptions) 1) Mass Spectrum a) Co effects as appropriate) b) Application of M (Rule of 13, N Rule, etc.) c) Fragmentation #1 (if possible). d) Fragmentation #2 (if possible). mment on M (there or not; note import of ionization technique if different than el; isotope Explain base peak, if possible; fragmentation to make some structural point is preferable, if possible; always use proper arrow notation to show how it happens 2) Infrared Spectrum a) Note major features regarding functional groups present, note anomalies of importance as appropriate b) Note lack of features as sign of possible absence of key functionalg 3) 'H-NMR Spectrum ment on number of different types of hydrogen relative to absorption signals a) Com b) Analyze integration ratios, if provided; connect to molecular for c) Explain chemical shifts relative to molecular structure features mula) Analyze splitting of absorption signals, insofar as is possible, relative to molecular structure ea ake sure your proposed structure is labeled appropriately (e. g. A, B, C.... and use thos features A, B. C designations to refer to different H's in designations to refer to different H's in your explanations to 3a-d above. e: It other information is given, e.g. an elemental analysis or a UV-Vis spectrum, it is general asent for a reason. Therefore, make sure you comment on that information in the context your proposed structure.
Solve the following holistic problem listing everything on the following checklist
General Checklist for Holistic Structure Problems (there are always exceptions) 1) Mass Spectrum a) Co effects as appropriate) b) Application of M (Rule of 13, N Rule, etc.) c) Fragmentation #1 (if possible). d) Fragmentation #2 (if possible). mment on M (there or not; note import of ionization technique if different than el; isotope Explain base peak, if possible; fragmentation to make some structural point is preferable, if possible; always use proper arrow notation to show how it happens 2) Infrared Spectrum a) Note major features regarding functional groups present, note anomalies of importance as appropriate b) Note lack of features as sign of possible absence of key functionalg 3) 'H-NMR Spectrum ment on number of different types of hydrogen relative to absorption signals a) Com b) Analyze integration ratios, if provided; connect to molecular for c) Explain chemical shifts relative to molecular structure features mula) Analyze splitting of absorption signals, insofar as is possible, relative to molecular structure ea ake sure your proposed structure is labeled appropriately (e. g. A, B, C.... and use thos features A, B. C designations to refer to different H's in designations to refer to different H's in your explanations to 3a-d above. e: It other information is given, e.g. an elemental analysis or a UV-Vis spectrum, it is general asent for a reason. Therefore, make sure you comment on that information in the context your proposed structure.
Patrina SchowalterLv2
27 Jul 2019