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13 Dec 2019

2. Make buoyancy corrections for the weights in part 1 to determine the real mass of each sample of water. Use the buoyancy correction equation, assuming the balance weights have a density of 8.0 g/mL. Use the density of water determined from the appendix (the temperature is 22°C). The Density of Water at 22 degrees Celsius is 0.9977735 (g/mL).

1. Using a 25-mL volumetric transfer pipet, pipet 25 mL of DI water into a dry, pre-weighed, conical flask or a beaker and weigh the sample. Use an analytical balance (± 0.0001 g) to make these weighings. Read and carefully follow the "Analytical Balance" instructions. Repeat 3 times. Calculate the average value of your measurements and the standard deviation.

Wvac = Wair + Wair [(0.0012/Do)-(0.0012/Dw)]

Wvac = weight in vacuum, g; Wair = weight in air, g

Do = density of object; Dw = density of weights

0.0012 = density of air

This table shows the results of the 25 mL transfer:

25-mL Trial #

Mass of flask

(without water)

Mass of flask

(with water)

Mass of the water

(Difference in masses)

1

48.0485 g

72.6685 g

24.6200 g

2

51.5100 g

76.2950 g

24.7850 g

3

55.2756 g

80.1296 g

24.8540 g

Average value: 24.5730 g

Standard Deviation: 0.0981733 g

This table shows the results of the 10 mL transfer:

10-mL Trial #

Mass of flask

(without water)

Mass of flask

(with water)

Mass of the water

(Difference in masses)

1

48.0167 g

57.9463 g

9.9295 g

2

52.0842 g

62.0142 g

9.9300 g

3

55.2745 g

65.2300 g

9.9555 g

Average Value: 9.9383 g

Standard Deviation: 0.12140 g (five significant figures within the mass of water).

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